H organic solvents: hexane, hexane tOAc mixtures, EtOAc, EtOAc eOH mixtures, MeOH, dichloromethane (Kim et al.b; Shin et al.; EstradaReyes et al); Extraction with diethyl ether and boiling methanol followed by cold storage ( ) and steam distillation (Weyerstahl et al); Headspace (Mazza and Kiehn ; W.H organic and natural solvents: hexane, hexane tOAc mixtures, EtOAc, EtOAc eOH mixtures, MeOH, dich